Pharmaceutical Drug Analysis 2da edición


Por Ashutosh Kar

Editorial: New Age Publications (Academic),India
Numero de Páginas: 564
ISBN-10 / ASIN: 8122415822
ISBN-13 / EAN: 9788122415827


The main purpose of this textbook is to discuss in an explicit and lucid manner several of the newer methods that now find rather wider application in the domain of pharmaceutical analysis. The basic principle of each technique is critically treated with emphasis on factors that directly affect its proper and judicious application to various analytical problems. An in-depth knowledge of these principles, instrumentations, modus operandi, experimental parameters, and sample preparation procedures in order to optimize the performance procedure of typical assay of pharmaceutical secondary products i.e., dosage forms, calculations etc., along with cognate assays from the Official Compendia have been included profusely.

Undergraduate and postgraduate students of pharmaceutical drug analysis, quality assurance chemists, industrial trainees, bulk-drug professionals and those in related disciplines earnestly requiring a substantial fundamental understanding and knowledge of the subject will certainly find this a much needed suitable compilation for reading and reference.

The broad coverage included in each of the selected analytical techniques would render Pharmaceutical Drug Analysis to be an useful source of ideas, inspiration for research, and developing newer practical solutions to problems in the ever expanding field of pharmaceutical analysis.

Contents:

Part I: GENERAL ASPECTS
Pharmaceutical Chemicals: Purity and Management Theory and Technique of Quantitative Analysis

Errors in Pharmaceutical Analysis and Statistical Validation


Part II: CHEMICAL METHODS
Titrimetric Methods: Acidimetry and Alkalimetry Aqueous Titrations, Non-Aqueous Titration

Redox Methods Permanganate, Dichromate and Ceric Sulphate Titration Methods, Iodimetric and Iodometric Titrations

Precipitation Methods-Argentometric Methods

Complexometric Methods-Complexometric Analysis

Gravimetric Methods-Gravimetric Analysis

Thermoanalytical Methods-Thermoanalytical Analysis

Miscellaneous Methods-Diazotization

Estimation of Phenols and Related Compounds

Karl Fisher Method for Determination of Water

Tertazolium Assay of Steroids


Part III: ELECTROCHEMICAL METHODS
Potentiometric Methods

Amperometric Methods


Part IV: OPTICAL METHODS
Refractometry

Polarimetry

Nephelometry and Turbidimetry

Ultraviolet and Absorption Methods

Infrared Spectrophotometry

Nuclear Magnetic Resonance Spectroscopy

Emission Spectroscopy

Flame Spectroscopy

Atomic Absorption Spectroscopy


Part V: ASSAY METHODS BASED ON SEPARATION TECHNIQUES
Liquid-Liquid Extraction

Thin Layer Chromatography (TLC)

Gas-Liquid Chromatography (GLC)

High Performance Liquid Chromatography (HPLC)

Size Exclusion Chromatography


Part VI: MISCELLANEOUS METHODS
Radioimmunoassay

Peso 3.3

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